Using English to Report Rendement
In chemistry, the
chemical yield, the yield of the reaction, or only the rendement refers to the
amount of reaction product produced in the chemical reaction. [1] Absolute
rendement can be written as weight in grams or in moles (molar yield). The
relative yield used as a calculation of the effectiveness of the procedure is
calculated by dividing the amount of product obtained in moles by the
theoretical yield in moles:
Rendemen fractional = rendemen actual / theoretical rendemenTo obtain a percentage yield, multiply the fractional yield by 100%.
One or more reactants in chemical reactions are often used redundantly. The
theoretical rendement is calculated based on the number of moles of the
limiting reagent. For this calculation, it is usually assumed that there is
only one reaction involved. The ideal chemical yield value (theoretical rendement) is 100%, a value highly
unlikely to be achieved in its practice. Calculate the percentage of rendement
that is by using the following equations percent rendemen = weight yield /
weight of yield divided by the sample weight multiplied by 100%.
We can learn with this practice :
ASETAT
/ CUKA ACID (CH3COOH)
WITH 0.1 N NaOH
WITH 0.1 N NaOH
Name : Novia Rahmiati
Date of practice :
I. Purpose
The purpose and objective of this practicum is for the practitioner to know and understand how to determine the level of acetic acid with 0.1 N NaOH.
II. Tools and reagents
Tools :
# Erlenmeyer 250 ml
# Pipette volume 10 ml + 25 ml
# Buret 50 ml
# Cup cup 100 ml
# Funnels
Reactor :
** NaOH 0.1 N
** Acetic acid (Vinegar)
** PP Indicators
Reaction:
NaOH + CH3COOH >>> CH3COONa + H2O
Tools :
# Erlenmeyer 250 ml
# Pipette volume 10 ml + 25 ml
# Buret 50 ml
# Cup cup 100 ml
# Funnels
Reactor :
** NaOH 0.1 N
** Acetic acid (Vinegar)
** PP Indicators
Reaction:
NaOH + CH3COOH >>> CH3COONa + H2O
III. Ways of working :
Clean and rinse buret with distilled water.
^^^
Bilasi and buret contents with 0.1 N NaOH solution until full and dihimpitka drawn (scale) zero.
^^^
Pipette 25 ml of acetic acid into 100 ml measuring flask, dilute to the line mark.
^^^
Beat the 12 x solution.
^^^
Pipette 10 ml aqueous solution into the erlenmeyer.
^^^
Spend 2 drops of PP indicator.
^^^
Titar with NaOH solution from burette to pink point of end.
^^^
Calculate the acetic acid level in% or g / l.
IV. Data and
calculations
BE = BM = 60
Final volume: 39.60 ml
Initial Volume: 0.00 ml -
Titration volume: 39.60 ml
Final volume: 39.50 ml
Initial Volume: 0.00 ml -
Titration volume: 39.50 ml
# Average titration volume = (39.60 + 39.50): 2 = 39.55 ml
#Chart of CH3COOH = X ml x N. NaOH x P x BE = 39.55 ml x 0.1N x (100 x 1000) x 60: 250 = 39.55 x 0.1 x 400 x 60 = 94.920 mg / l = 94.920 g / l
#% CH3COOH = acetic acid concentration (g / l) x 100%
1000 x BJ (considered 1)
= 94.920 x 100%
1000
= 9,492%
BE = BM = 60
Final volume: 39.60 ml
Initial Volume: 0.00 ml -
Titration volume: 39.60 ml
Final volume: 39.50 ml
Initial Volume: 0.00 ml -
Titration volume: 39.50 ml
# Average titration volume = (39.60 + 39.50): 2 = 39.55 ml
#Chart of CH3COOH = X ml x N. NaOH x P x BE = 39.55 ml x 0.1N x (100 x 1000) x 60: 250 = 39.55 x 0.1 x 400 x 60 = 94.920 mg / l = 94.920 g / l
#% CH3COOH = acetic acid concentration (g / l) x 100%
1000 x BJ (considered 1)
= 94.920 x 100%
1000
= 9,492%
V. Discussion:
In diluting the standard solution must be precisely coined zero (scale) in
order to keep acetic acid content or unchanged. Then the solution should be
shaken at least 12x for a homogeneous solution and the final result is
appropriate. In this experiment, the indicator used is penolftalin (PP) with a
pH trajectory between 8.2 to 10, because the guitar is a strongly alkaline
NaOH. In practice, it should be done 2 times the experiment so that the results
more accurate in determining levels. The difference between the 2 experiments
is a maximum of 0.1 ml. In doing the titration should be careful because if
less will only affect the final result. The result of end pointing should be
pink because at that time the solution is neutral.
VI. Conclusion:
Thus, CH3COOH levels of 94.920 g / l or 9.492%
BalasHapusWhat is the function of the pp indicator? And in another practice can use other indicators?..
HapusThe pp indicator is used to distinguish the color, wherein the acidic conditions indicator is colorless and under basic conditions turns pink, in addition to this experiment, the indicator can be used in the experimental identification of acid and base of a solution
BalasHapusYour opinion, what is the point we predict the rendement?
HapusThe purpose of doing the prediction is to be the initial hypothesis before the experiment, so the hypothesis we will make as a comparison with the final results of the experiment, used as a discussion in a problem and as one part of thinking saintific
What is the benefit of rendement on this experiment?
BalasHapusFrom this experiment the rendement obtained can be evaluated to make the experiment failed, and praktikan can train skill in doing experiment
Hapus
BalasHapusplease explain to me about prediction from your rendement ?thanks
CH3COONa is the predicted reaction result, where the reaction result will be pink, and 9,492% is the result of its rendement
HapusPlease give your example calculation with the concept of rendement.
BalasHapus#Chart of CH3COOH = X ml x N. NaOH x P x BE = 39.55 ml x 0.1N x (100 x 1000) x 60: 250 = 39.55 x 0.1 x 400 x 60 = 94.920 mg / l = 94.920 g / l
Hapus#% CH3COOH = acetic acid concentration (g / l) x 100%
1000 x BJ (considered 1)
= 94.920 x 100%
1000
= 9,492%
why Clean and rinse buret with distilled water.?
BalasHapusbecause if we clean it with distilled water it can't be contaminated
Hapus